Journal of the American Chemical Society p. 1746 - 1752 (1994)
Update date:2022-08-03
Topics: Solid-phase synthesis Silicon-derived linkage agent 4-[1-hydroxy-2-(trimethylsilyl)ethyl]benzoic acid Fmoc/t-Bu strategy C-terminal peptide acids
Chao, Hann-Guang
Bernatowicz, Michael S.
Reiss, Paul D.
Klimas, Clifford E.
Matsueda, Gary R.
Tryptophan alkylation by resin-derived carbocations and formation of diketopiperazine are two major yield reducing side reactions observed in Fmoc/t-Bu based solid-phase peptide synthesis. With the development of a versatile silicon-based linkage agent, "
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