Journal of Organic Chemistry p. 6192 - 6201 (2017)
Update date:2022-07-30
Topics:
He, Lisi
Yang, Xinkan
Tsui, Gavin Chit
A domino hydroboration/trifluoromethylation (formal hydrotrifluoromethylation) of alkynes using the fluoroform-derived [CuCF3] reagent is achieved. Synthetically useful (E)-alkenyl-CF3 building blocks and 1,1-bis(trifluoromethyl)-substituted alkenes can be prepared under ambient conditions in one pot/one step from alkynes. The ultimate source of CF3 is the inexpensive industrial waste fluoroform.
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