Journal of Organic Chemistry p. 4206 - 4210 (1994)
Update date:2022-08-03
Topics:
Lei, Haiyan
Stoakes, Mark S.
Herath, Kamal P. B.
Lee, Jinho
Schwabacher, Alan W.
A new amphiphilic bis-amino acid has been designed and its convergent, asymmetric synthesis achieved in differentially protected form.A convenient preparation of iodophenylalanine, a generally useful starting material, is disclosed.Sequential palladium-catalyzed couplings of aryl iodides to phosphinate lead directly to the target protected bis-amino acid.Controlled peptide coupling of the new bis-amino acid is also demonstrated.
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Doi:10.1007/s00706-018-2152-8
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(1968)Doi:10.1039/C8SC01763H
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(1994)
