Tetrahedron Letters p. 1411 - 1412 (1997)
Update date:2022-09-26
Topics:
Agrofoglio, Luigi A.
Jacquinet, Jean-Claude
Lancelot, Gerard
The preparation of 13C-labeled ribonucleosides starting from D-[13D6]glucose in 45% overall yield is described. The key of this short synthetic way is the dehomologation of di-O-isopropylidene hexofuranose 2 with periodic acid and NaBH4 that afforded stereoselectively the labeled ribofuranose derivative 3 in high yield.
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