Journal of Fluorine Chemistry p. 5 - 6 (1994)
Update date:2022-08-02
Topics:
Iseki, Katsuhiko
Kuroki, Yoshichika
Nagai, Takabumi
Kobayashi, Yoshiro
The hydrogenation of (E)-2-(trifluoromethyl)alk-2-en-1-ols catalyzed by Ru-BINAP and Rh-BINAP has been carried out with good enantiomeric excess (71percent-83percent ee).Ru-BINAP-catalyzed hydrogenation converted 2-trifluoromethylacrylic acid to the corresponding saturated acid, the esterification and reduction of which gave optically active 2-(trifluoromethyl)propan-1-ol in 80percent ee.
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