Synthesis p. 1445 - 1449 (1994)
Update date:2022-08-03
Topics:
Zeltner
Olk
Wagner
Olk
An efficient method for the preparation of the unsymmetrically substituted 1,3-dithiole-2-thione-4,5-dithiolate (dmit) is reported. Its application is demonstrated by obtainment of various 1,3-dithiole-2-thione-4-thiolate-5-thioesters and ethers. Starting from these compounds an expedient route to novel unsymmetrical crown compounds and tetrathiafulvalenes is shown.
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Doi:10.1021/jo00881a017
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