Synthesis of Complexes (1+) (L = Primary, Secondary or Tertiary Amine). Crystal Structure of *CH2Cl2

DOI: 10.1039/DT9950001251

Source and publish data:

Journal of the Chemical Society, Dalton Transactions p. 1251 - 1254 (1995)

Update date:2022-08-05

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Authors:

Vicente, Jose

Chicote, Maria-Teresa

Guerrero, Rita

Jones, Peter G.

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Article abstract of DOI:10.1039/DT9950001251

The 1:1 reaction of (Hacac = acetylacetone) with ammonium salts X (X = CF3SO3, L = 2-nitroaniline, 4-methoxyaniline, NHPh2 or NHEt2; X = ClO4, L = NMe3) in diethyl ether gave complexes X and acetylacetone.The crystal structure of was determined; orthorhombic, space group P2₁2₁2₁, a = 9.498(2), b = 10.322(2), c = 26.154(4) Angstroem, wR(F²) 0.091.The gold atom is linearly co-ordinated to both ligands and no intermolecular Au..Au contacts exist.

Full text of DOI:10.1039/DT9950001251

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