Journal of the Chemical Society, Dalton Transactions p. 2177 - 2178 (1996)
Update date:2022-08-06
Topics:
Hui, Bernard Kwok-Man
Wong, Wing-Tak
The cluster [Os3(CO)10(NCMe)2] reacted with [N(PPh3)2]NO2 in CH2Cl2 to give a novel red-orange complex [N(PPh3)2][Os3(CO)10(μ-η 2-NO2)] in moderate yield, which underwent protonation with HBF4·Et2O in CH2Cl2 to give the neutral complex [Os3(μ-H)(CO)10(μ-η2-NO2)] in high yield; X-ray crystal-structure analyses have shown that both clusters contain a μ-η2-bridging nitrite ligand.
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Doi:10.1080/00945719608004340
(1996)Doi:10.1002/jhet.840
(2013)Doi:10.1016/0277-5387(95)00567-6
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(1996)
