Heterocycles p. 1821 - 1824 (2006)
Update date:2022-07-30
Topics:
Isoda, Takeshi
Tamai, Satoshi
Kumagai, Toshio
Nagao, Yoshimitsu
An efficient method for the synthesis of 3-mercapto-1-(1,3-thiazolin-2-yl)azetidine (1) is described. This thiol synthesis was achieved in 3 steps from readily available 3-methanesulfonyloxyazetidine via key intermediates, Bunte salts (3 and 5). The final step was enabled to proceed under mild conditions using the benzylthiol-mediated cleavage of the S-S bond in the Bunte salt (3).{A figure is presented}.
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Doi:10.1016/j.tetlet.2006.03.142
(2006)Doi:10.1002/hlca.19830660834
(1983)Doi:10.1016/j.tetlet.2006.03.051
(2006)Doi:10.1016/j.jcat.2015.10.001
(2015)Doi:10.1016/j.tetlet.2006.03.096
(2006)Doi:10.1021/ja061970a
(2006)