Journal of Organometallic Chemistry p. 29 - 36 (1995)
Update date:2022-08-02
Topics:
Ruehlmann, K.
Jaehnichen, S.
Scheim, U.
Scheller, D.
Keidel, F.
A series of 2-functional 1,3-dioxa-2,4,7-trisilacycloheptanes was synthesized and characterized by means of 29Si NMR spectroscopy, gas chromatography, high performance liquid chromatography and gas chromatography-mass spectrometry.The signals were assigned to the various configurational isomers.This assignment was confirmed by independent synthesis of individual isomers.The sequence of the NMR signals of the all-cis and trans-trans isomers required for the determination of stereochemistry was found to be the same as that of the respective cyclotrisiloxanes.Keywords: Cyclosiloxanes; Synthesis; Spectroscopic characterization
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