Tetrahedron Letters p. 6133 - 6136 (1996)
Update date:2022-07-29
Topics:
Sujino, Keiko
Yoshida, Tomoyasu
Sugimura, Hideyuki
A straightforward approach for the synthesis of 2',3'-unsaturated nucleosides starting from 2-deoxyribose is described. This novel route involves two new methods; (1) preparation of 2-deoxy-1-thioribofuranoside by direct condensation of 2-deoxyribose and thiophenol, (2) formation of the nucleoside skeleton by the direct coupling of 2,3-unsaturated 1-thiopentofuranoside with pyrimidine bases.
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