Organic Letters p. 5368 - 5371 (2017)
Update date:2022-08-05
Topics:
Davidson, Samuel J.
Pearce, A. Norrie
Copp, Brent R.
Barker, David
The first total synthesis of (-)-bicubebin A, and two previously unreported dilignans, (-)-bicubebin B and (+)-bicubebin C has been achieved through the dimerization of (-)-cubebin, confirming the structure and absolute stereochemistry of (-)-bicubebin A. Analysis of the data for (-)-bicubebin B showed it matched that of reported compound (-)-cis-cubebin. The NMR data of the subsequently synthesized proposed structure of cis-cubebin confirmed that its original proposed structure was incorrect.
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