Tetrahedron Letters p. 7391 - 7394 (1997)
Update date:2022-09-26
Topics: Synthesis Compound Experimental
Torii, Sigeru
Hase, Tomoyuki
Kuroboshi, Manabu
Amatore, Christian
Jutand, Anny
Kawafuchi, Hiroyuki
Terminal-biradical compounds 1 having two N-oxyl groups connected with conjugated π-systems were synthesized by (1) addition of magnesium acetylide to 4-oxo-TEMPO, followed by dehydration, or (2) cross-coupling between acetylene and vinyl triflate derived from 4-oxo-TEMPO.
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