Carbohydrate Research p. 2290 - 2293 (2011)
Update date:2022-08-04
Topics:
Zhang, Jianbo
Fu, Jie
Si, Wenshuai
Wang, Xiaohu
Wang, Zhongfu
Tang, Jie
Commercially available zinc dust in the presence of ammonium chloride in acetonitrile at reflux removes the 2,2,2-trichloroethyl (TCE) group at anomeric centers with excellent yields (>95%) in short reaction times. This present method is easily implemented on substrates containing acyl and benzyl groups and large-scale reactions also proceed in high yield.
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