Chemistry Letters p. 651 - 652 (1998)
Update date:2022-08-02
Topics:
Ito, Shigekazu
Yoshifuji, Masaaki
The phenylthio group was introduced to the sterically protected phosphaethene-system and 1-(phenylthio)-2-(2,4,6-trit-butylphenyl)-2-phosphaethenyllithium was generated. It has been shown that the lithium reagent behaves like a haloderivative, in terms of elimination, metalation, and coupling reaction, while the E/Z isomerization was observed for the phenylthio-derivative, and a 1,4-diphospha-1,3-butadiene as an oxidative coupling product was analyzed by X-ray.
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