Tetrahedron Letters p. 7135 - 7138 (1998)
Update date:2022-07-29
Topics:
Kurata, Hiroyuki
Monden, Masahisa
Kawase, Takeshi
Oda, Masaji
Tetrakis(2-thienyl)allene was synthesized as an acid-sensitive tetraarylallene by dehydration of the corresponding tetrathienylallyl alcohol with anhydrous copper(II) sulfate. This electron-rich allene forms a remarkably stable tetrathienylallyl cation by protonation, undergoes Diels- Alder reaction with tetracyanoethylene, and is capable of tetrafold lithiation and functionalization.
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