
Synthesis p. 1590 - 1592 (1998)
Update date:2022-08-04
Topics:
Blanco, Jose M.
Caamano, Olga
Fernandez, Franco
Garcia-Mera, Xerardo
Lopez, Carmen
Rodriguez-Borges, Jose E.
Hergueta, Antonio R.
Glyoxylates of three chiral alcohols were conveniently prepared by reaction of the alcohol with oxalyl chloride followed by reduction of the resulting alkoxy oxalyl chloride with tributyl- tin hydride. The products were isolated in 75-80% yield by straightforward flash chromatography.
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Doi:10.1021/jm00303a600
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(1998)