Tetrahedron Letters p. 9573 - 9574 (1998)
Update date:2022-08-03
Topics:
Harrowven, David C.
Hannam, Joanne C.
The paper describes a short synthesis of α-herbertenol. Key features are the addition of dihyropyranone 5 to an aryllithium to give 1,5-diketone 7; a titanium(O) mediated cyclisation of 7 to diol 8 and a sequential methylation of 8 to herbertenol methyl ether 9.
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