Preparation of dendrons with peripheral fullerene units

DOI: 10.1016/S0040-4039(98)02378-8

Source and publish data:

Tetrahedron Letters p. 269 - 272 (1999)

Update date:2022-08-03

Topics: Synthesis Characterization Yield Protecting group Michael addition Purification Conjugation Workup Reaction Monitoring Coupling Reaction Click Chemistry Fullerene Stoichiometry Sonication

Authors:

Nierengarten, Jean-Francois

Felder, Delphine

Nicoud, Jean-Francois

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Article abstract of DOI:10.1016/S0040-4039(98)02378-8

Highly soluble dendritic branches with fullerene subunits at the periphery and a carboxylic acid function at the focal point have been prepared by a convergent approach, using successive DCC-mediated esterifications followed by cleavage of a t-butyl ester moiety under acidic conditions.

Full text of DOI:10.1016/S0040-4039(98)02378-8

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Product name:bis{[3,5-bis(octyloxy)phenyl]methyl} 11''-(carboxymethoxy)-4'',15''-dioxo-3',3''-(methanoxymethano[1,3]benzenomethanoxymethano)-3'H,3''H-dicyclopropa[1,9:3,15][5,6]fullerene-C₆₀-I_h-3',3''-dicarboxylate

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