Acta Crystallographica, Section C: Crystal Structure Communications p. 744 - 748 (1999)
Update date:2022-08-04
Topics:
Lo, Kong Mun
Kumar Das
Ng, Seik Weng
Hook, James M.
Carboxylate bridges link the two independent molecules of triphenyltin N,N-diethylthiocarbamoylthioacetate, (I), and the four independent molecules of triphenyltin N-methyl-N-phenylthiocarbamoylthioacetate, (II), into linear chains whose Sn atoms show trans-trigonal-bipyramidal coordination, i.e. (I) is catena-poly[triphenyltin-μ-(N,N-diethylthiocarbamoylthioacetato-O:O′)], [Sn(C6H5)3(μ-C7H 12NO2S2)]n, and (II) is catena-poly[triphenyltin-μ-(N-methyl-N-phenylthiocarbamoylthioacetato-O: O′)], [Sn(C6H5)3(μ-C10H 10NO2S2)]n. Triphenyltin N,N-tetramethylenethiocarbamoylthioacetate {or triphenyl(N,N-tetramethylenethiocarbamoylthioacetato-O)tin, [Sn(C6H5)3(C7H10-NO 2S2)]} exists as a monomeric tetrahedral molecule.
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