Journal of the Chemical Society, Dalton Transactions p. 2011 - 2013 (1981)
Update date:2022-08-03
Topics:
Millington, Peter L.
Sowerby, D. Bryan
An X-ray analysis of the title compound shows slightly distorted trigonal-bipyramidal geometry about the central atom is contrast to square-pyramidal co-ordination in the related SbPh5.The heavy-atom method was used with X-ray diffractometer data and refinement by full-matrix least squares converged at R 0.036 for 3367 reflections.Crystals are monoclinic, space group P21/n, with a=10.488(5), b=16.561(8), c=13.503(6) Angstroem, β=92.16(2) deg, and Z=4.
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