Tetrahedron Letters p. 6465 - 6468 (1999)
Update date:2022-08-04
Topics:
Obika, Satoshi
Andoh, Jun-ichi
Sugimoto, Tomomi
Miyashita, Kazuyuki
Imanishi, Takeshi
A bicyclic 3'-azido-3'-deoxythymidine (AZT) analogue with a locked N- conformation, 3'-azido-3'-deoxy-2'-O,4'-C-methylene-5-methyluridine (1a), and its 3'-amino derivative, 3'-amino-3'-deoxy-2'-O,4'-C-methylene-5- methyluridine (1b), were successfully synthesized from D-glucose. The conformation of 1a was also discussed by means of 1H NMR measurements and a molecular modeling (PM3) study.
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