Tetrahedron p. 3711 - 3716 (1989)
Update date:2022-08-02
Topics:
Turner, Walter V.
Gaeb, Siegmar
Contrary to a previous report, there is no solvent-dependent selectivity to either of the double-bond-dechlorinated derivatives when Bromodan is irradiated in hexane or methanol.The 7-dechlorinated derivative formed on photolysis in triethylamine is debrominated on further irradiation. 13C chemical shifts and longe-range C-H coupling constants indicate that the structural assignment of the double-bond-dechlorinated isomers mest be reversed.
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