Tetrahedron Asymmetry p. 3601 - 3614 (1999)
Update date:2022-08-04
Topics:
Chauret, Denise C.
Chong, J. Michael
Ye, Qing
Asymmetric epoxidation of (E)-3-trialkylsilyl-2-propen-1-ols gives the expected epoxides with high enantioselectivity. Ring opening reactions of these epoxides with organocopper reagents furnishes 1,2-diols which are readily cleaved with Pb(OAc)4 to afford α-silyl aldehydes with no detectable loss of stereochemistry.
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