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which gave 61 mg of 81SbF26 (77%) as an off-white
powder. Cooling of the mother liquor to 2308C, gave
ca. 8 mg of white crystals, which were identified by
X-ray diffraction.
• A toluene solution of 6 was degassed in vacuo and then
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solvent resulted in an off-white oil, which contained,
according to its 31P-NMR spectrum, only 81Cl2
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Supplementary data
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Supplementary data are available from the Cambridge
Crystallographic Data Centre, 12 Union Road, Cambridge
CB2 1EZ, UK on request, quoting the deposition numbers
117254 (compound 3c) and 117255 (5).
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Acknowledgements
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We want to express our gratitude to Prof. Wolfgang
Beck for his continuous interest and support and to Dr.
Margaret Crawford for reading and correcting this manu-
script. Financial support by the Deutsche Forschungs-
gemeinschaft and the Fonds der Chemischen Industrie is
greatly appreciated.
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