Tetrahedron p. 14261 - 14268 (1999)
Update date:2022-08-05
Topics:
Crich, David
Xiaolin, Hao
Lucas, Mathew
The synthesis of a minimally fluorous (52% F) diaryl diselenide is described. On reduction in situ with tributylstannane this diselenide provides a fluorous selenol which is effective in inhibiting a range of stannane-mediated radical rearrangements, including a cyclopropylcarbinyl ring opening. A method for the recovery of the fluorous diselenide involving continuous extraction in a modified, cooled continuous extractor is described.
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Doi:10.1021/ja00707a019
(1970)Doi:10.1016/j.carbpol.2016.01.069
(2016)Doi:10.1016/S0022-1139(99)00186-4
(2000)Doi:10.1021/jo990964c
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(1999)Doi:10.1002/(SICI)1521-3765(20000103)6:1<162::AID-CHEM162>3.0.CO;2-9
(2000)
