Tetrahedron Letters p. 4487 - 4488 (1997)
Update date:2022-08-05
Topics:
Mashraqui, Sabir H.
Nivalkar, Kishor R.
Synthesis of the first [2.2] benzofused heterophane 8 is described via photodecarboxylation of bislactone 7. Dynamic 1H NMR studies suggest that 8 is conformationally rigid whereas 7 is conformationally mobile on the NMR time scale.
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