A facile one-pot synthesis of 2,3'-anhydro-2'-deoxyuridines via 3'-O-imidazolylsulfonates

Article abstract of DOI:10.1080/00397910008086944

Continued interests in the novel synthetic methods of the pivotal compound, 2,3'-anhydro-2'-deoxyribonucleosides (7) uncovered a facile one-pot conversion of 5 with 1,1'-sulfonyldiimidazole in basic conditions to 7 with almost quantitative yields (91-99%).

Full text of DOI:10.1080/00397910008086944

This article was downloaded by: [Ams/Girona*barri Lib]
On: 17 October 2014, At: 02:12
Publisher: Taylor & Francis
Informa Ltd Registered in England and Wales Registered Number: 1072954
Registered office: Mortimer House, 37-41 Mortimer Street, London W1T 3JH,
UK
Synthetic Communications: An
International Journal for Rapid
Communication of Synthetic
Organic Chemistry
Publication details, including instructions for
authors and subscription information:
http://www.tandfonline.com/loi/lsyc20
A Facile One-Pot Synthesis of
2,3′-Anhydro-2′-Deoxyuridines
via 3′-O-Imidazolylsulfonates
Zaesung No a , Dong Seong Shin a , Bok Ju Song a ,
Mija Ahn a & Deok-Chan Ha b
a Bioorganic Science Division , Korea Research
Institute of Chemical Technology , P.O. Box 107,
Yusong, Taejon, 305-600, Korea
b Department of Chemistry , Korea University ,
Anam-Dong, Seoul, 136-701, Korea
Published online: 04 Dec 2007.
To cite this article: Zaesung No , Dong Seong Shin , Bok Ju Song , Mija Ahn & Deok-
Chan Ha (2000) A Facile One-Pot Synthesis of 2,3′-Anhydro-2′-Deoxyuridines via 3′-O-
Imidazolylsulfonates, Synthetic Communications: An International Journal for Rapid
Communication of Synthetic Organic Chemistry, 30:21, 3873-3882
To link to this article: http://dx.doi.org/10.1080/00397910008086944
PLEASE SCROLL DOWN FOR ARTICLE
Taylor & Francis makes every effort to ensure the accuracy of all the
information (the “Content”) contained in the publications on our platform.
However, Taylor & Francis, our agents, and our licensors make no
representations or warranties whatsoever as to the accuracy, completeness,
or suitability for any purpose of the Content. Any opinions and views
expressed in this publication are the opinions and views of the authors, and

are not the views of or endorsed by Taylor & Francis. The accuracy of the
Content should not be relied upon and should be independently verified with
primary sources of information. Taylor and Francis shall not be liable for any
losses, actions, claims, proceedings, demands, costs, expenses, damages,
and other liabilities whatsoever or howsoever caused arising directly or
indirectly in connection with, in relation to or arising out of the use of the
Content.
This article may be used for research, teaching, and private study purposes.
Any substantial or systematic reproduction, redistribution, reselling, loan,
sub-licensing, systematic supply, or distribution in any form to anyone is
expressly forbidden. Terms & Conditions of access and use can be found at
http://www.tandfonline.com/page/terms-and-conditions