Tetrahedron p. 1180 - 1185 (2019)
Update date:2022-08-02
Topics:
Wang, Yingying
Zhou, Yang
Lei, Min
Hou, Jinjun
Jin, Qinghao
Guo, Dean
Wu, Wanying
A straightforward and general method has been developed for the synthesis of phthalimide derivatives from 2-iodobenzamides and PPh3/I2/HCOOH in the presence of a catalytic amount of Pd(OAc)2. The reaction results demonstrate that PPh3/I2/HCOOH is a facile, efficient and safe CO source. The whole process is carried out in toluene at 80 °C and furnishes the desired products in good to excellent yields.
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Doi:10.1002/1521-4184(200101)334:1<21::AID-ARDP21>3.0.CO;2-W
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(2021)
