Tetrahedron Letters p. 3407 - 3410 (1996)
Update date:2022-08-03
Topics: Oxidation Regioselectivity Column chromatography Yield NMR spectroscopy Catalyst Enantiomeric excess (ee) TLC (thin-layer chromatography) Workup Reaction Conditions Stereoselectivity Reaction Monitoring Quenching Chiral Ligand Dihydroxylation Sharpless asymmetric dihydroxylation Vicinal diols Solvent system
Donohoe, Timothy J.
Garg, Rina
Moore, Peter R.
The preparation and dihydroxylation (OsO4) of a series of conformationally constrained allylic alcohols is described. By using dichloromethane as solvent, the selectivity that favours the anti triol is substantially reduced by hydrogen-bonding
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