Chemical Communications p. 14543 - 14546 (2015)
Update date:2022-08-04
Topics:
Cho, Beom Shin
Chung, Young Keun
A protocol involving facile sequential C(sp3)-H and C(sp2)-H activation reactions of 3-alkylbenzofurans catalyzed by Pd(OAc)2 in the presence of pivalic acid, silver salt, and tricyclohexylphosphine 'on water' was developed. Aryl iodides were used as substrates in a tandem bisarylation reaction to generate 3-arylalkyl-2-arylbenzofurans in moderate to high yields at room temperature. The reaction revealed in this study is a rare example of consecutive C(sp3)-H and C(sp2)-H bond activation under mild reaction conditions.
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