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Convenient Synthesis of Chiral 5-Amino-1,3-Dioxanes Built on Some 1-p-Nitrophenylserinols Skeletons

DOI: 10.1515/HC.2001.7.6.593

Source and publish data:

Heterocyclic Communications p. 593 - 598 (2001)

Update date:2022-09-26

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Authors:

Darabantu, MirceaDarabantu, Mircea

Maiereanu, CarmenMaiereanu, Carmen

Ple, GerardPle, Gerard

Berghian, CameliaBerghian, Camelia

Condamine, EricCondamine, Eric

Ramondenc, YvanRamondenc, Yvan

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Article abstract of DOI:10.1515/HC.2001.7.6.593

A simple and rapid methodology for the synthesis of the title compounds is described in order to access polychiral (enantiomerically pure) 5-aminodioxanes in satisfactory yields. The reaction of two nitrophenylserinols with two versatile carbonyl electrophiles (formaldehyde and glyoxal) in very strong acidic conditions (96% H2SO4) is discussed together with the limitations of the method.

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Full text of DOI:10.1515/HC.2001.7.6.593

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Download Date | 6/16/15 1:24 AM  
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Download Date | 6/16/15 1:24 AM  
Brought to you by | Purdue University Libraries  
Authenticated  
Download Date | 6/16/15 1:24 AM  
Brought to you by | Purdue University Libraries  
Authenticated  
Download Date | 6/16/15 1:24 AM  
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Products guided by the article

Product name:(2R,2'R,4S,4'S,5S,5'S)-5-amino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane

Cas No:440368-60-5

440368-60-5

R&D Labs maybe for 440368-60-5

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