Journal of the Chemical Society. Perkin Transactions 1 (2001) p. 2198 - 2203 (2002)
Update date:2022-08-04
Topics:
Porres, Laurent
Deleuze, Herve
Landais, Yannick
Polymer beads have been prepared by photocationic suspension polymerisation of 2-(aryldimethyl)silyl ethers in perfluorooctane in the course of our studies on polymer-supported desymmetrisation of 1-silacyclohexa-2,5-dienes. Good yields of 100-200 μm beads of satisfactory shape have been obtained using a perfluorinated co-polymer as stabilising agent. These beads have no permanent porosity although they have a high nominal cross-linking level. Their swelling in common organic solvents is comparable with those of Merrifield or TentaGel gel-type resins.
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