Journal of Organic Chemistry p. 836 - 839 (1994)
Update date:2022-08-03
Topics:
Uccello-Barretta, Gloria
Balzano, Federica
Caporusso, Anna Maria
Salvadori, Piero
The heptakis(2,3,6-tri-O-methyl)-β-cyclodextrin (TRIMEB) has been successfully used as convenient chiral solvating agent to determine the enantiomeric composition of chiral trisubstituted allenes by 1H NMR spectroscopy: the analysis of the effect of the molar ration TRIMEB/allene, temperature, and nature of the solvent allowed us to optimize the experimental conditions to enhance the separation between the signals of the two enantiomers of each allene.
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