Synlett p. 2339 - 2344 (2016)
Update date:2022-08-04
Topics:
Chen, Sihai
Li, You
Chen, Jinyang
Xu, Xinhua
Su, Lebin
Tang, Zhi
Au, Chak-Tong
Qiu, Renhua
Thioamides can be generated at 100 °C in high yield through the reaction of 1,2-dibenzyldisulfane with difurfuryldisulfide using iodine as oxidant and DMSO as solvent. The protocol is metal- and additive-free, providing a convenient and economical way for the synthesis of various kinds of thioamides under mild conditions.
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