Phosphorus, Sulfur and Silicon and the Related Elements p. 121 - 140 (1996)
Update date:2022-08-05
Topics:
Bode, Katrin
Klingebiel, Uwe
Witte-Abel, Henning
Gluth, Matthias
Noltemeyer, Mathias
Herbst-Irmer, Regine
Schaefer, Martina
Shomaly, Walid
Bulky fluorosilanes react with monolithiated hydrazine to give the stable mono(silyl)hydrazines H2N-NHR 1-3 <(R = Si(CMe3)2Me (1), R = Si(CMe3)2Ph (2), R = SiCMe3(CHMe2)2 (3)>.In a condensation reaction the symmetric bis(silyl)hydrazines 4 and 5 are obtained by 2 and 3 losing hydrazine.The reaction of lithiated 1, 2 and 3 with fluorosilanes leads to the formation of the asymmetric bis(silyl)hydrazines RHN-NHR', 6-10
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