Tetrahedron p. 4479 - 4484 (1996)
Update date:2022-08-05
Topics:
Raina, Sushil
Singh, Vinod K.
An efficient asymmetric synthesis of 5-hexadecanolide from a chiral epoxide is described. Both the enantiomeric forms of the chiral epoxide are easily available from mannitol and ascorbic acid. The key step in the synthesis is the formation of δ-lactone from δ-hydroxy acetal using m-CPBA and BF3-OEt2.
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