Advanced Synthesis and Catalysis p. 940 - 946 (2016)
Update date:2022-08-04
Topics: Column chromatography NMR spectroscopy Arylation Reaction Conditions Diaryliodonium salts 2-Substituted cyanoacetates
Qian, Xiaofei
Han, Jianwei
Wang, Limin
A transition metal-free direct arylation of 2-substituted cyanoacetates with diaryliodonium salts was developed. With this approach, a wide range of α-tolunitrile derivatives has been synthesized in good to excellent yields of 45-92%. Furthermore, the practicability of this approach is further manifested in the synthesis of a related bioactive agent of glutarimide.
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