Journal of Organometallic Chemistry p. 219 - 224 (1996)
Update date:2022-07-30
Topics:
Sanders, Richard
Mueller-Westerhoff, Ulrich T.
We reported in 1993 an efficient synthesis of ferrocene and ruthenocene mono-and dialdehydes which suggested the first truly specific monolithiation of these two metallocenes (U.T. Mueller-Westerhoff, Z. Yang and G. Ingram, J. Organomet. Chem., 463 (1993) 163). Unfortunately, these results were based on inappropriate experimental methods. We have now meticulously analyzed a wide spread of reaction conditions and have concluded that an effective monolithiation of ferrocene and of ruthenocene is possible, but not under the previously described reaction conditions.
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