Chemistry Letters p. 927 - 930 (1980)
Update date:2022-08-04
Topics: Reaction Preparation
Mitsunobu, Oyo
Kimura, Junji
Shimizu, Tatsuhiko
Kawashima, Atsushi
The reaction of ethoxycarbonylmethylenetriphenylphosphorane with aci-nitroesters derived from 2,6-di-t-butyl-4-nitrophenol and alcohols afforded α,β-unsaturated carboxylic esters.When mono-aci-nitroester of 1,3-butanediol or 1,6-hexanediol was used, (E)-ethyl 5-hydroxy-2-hexenoate or (E)-ethyl 8-hydroxy-2-octenoate was obtained.
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Doi:10.1016/S0008-6215(00)84631-5
(1979)Doi:10.1016/S0040-4039(00)92790-4
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(1986)Doi:10.1007/s10562-015-1515-6
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(2018)
