Direct Hydride/Silyl Exchange
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3
˚
˚
c ϭ 13.3894(4) A, β ϭ 99.620(1)°, V ϭ 1736.36(8) A , Z ϭ 4, d ϭ
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radiation and graphite monochromator, µ(Mo-Kα) ϭ 1.737 mmϪ1
,
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crystal size 0.30 ϫ 0.30 ϫ 0.08 mm, T ϭ 120(2) °C, data-collection
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metry-independent reflections with I Ͼ 2σ(I), multi-scan absorp-
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GOF ϭ 1.041. CCDC-219856 (6) and -190915 (8) contain the sup-
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obtained free of charge at www.ccdc.cam.ac.uk/conts/retriev-
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Support from the Russian Foundation for Basic Research for GIN
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Received March 10, 2003
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G. I. Nikonov, L. G. Kuzmina, J. A. K. Howard, Organometall-
Early View Article
ics 1997, 16, 3723.
Published Online December 12, 2003
Eur. J. Inorg. Chem. 2004, 771Ϫ775
2004 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim
775