Helvetica Chimica Acta p. 2030 - 2032 (1985)
Update date:2022-09-26
Topics:
Andrejevic, Vladimir
Bjelakovic, Mira
Mihailovic, Milan M.
Mihailovic, Mihailo Lj.
Unsubstituted medium-ring 1,2-epoxycycloalkanes and certain vic-epoxyalkanes are reduced to the corresponding alcohols very slowly when LiAlH4 alone is used as reducing agent.However, the combination of LiAlH4 and AlCl3, in a 2:1 molar ratio (with respect to 1 mol-equiv. of epoxide) used in refluxing Et2O, greatly enhances these reductions, rendering them of interest for practical purposes.
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