Helvetica Chimica Acta p. 315 - 319 (1980)
Update date:2022-08-03
Topics: SYNTHESE Ausbeute NMR-Spektroskopie Katalysator 8-Hydroxy-2-methyl-1,2,3,4-tetrahydroisochinolin Reaktionsmechanismus Charakterisierung Massenspektrometrie Reaktionsoptimierung Mechanistische Studien
Gray, Robert W.
Dreiding, Andre S.
Vilsmeier formylation of N-<2-(3,5-dimethoxyphenyl)ethyl>-trifluoroacetamide (5) yielded the aldehyde 6, which under mild basic conditions was hydrolyzed to 7 and cyclized to 6,8-dimethoxy-3,4-dihydroisoquinoline (3).Methylation of 3 and reduction of the
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Doi:10.1016/S0022-328X(00)83515-9
(1980)Doi:10.1021/jm00181a012
(1980)Doi:10.1021/acs.orglett.5b01628
(2015)Doi:10.1016/j.ica.2004.02.003
(2004)Doi:10.1021/jo00205a020
(1985)Doi:10.1021/op020060k
(2002)