Tetrahedron Letters p. 2275 - 2278 (1988)
Update date:2022-08-05
Topics:
Ok, Hyun
Caldwell, Charles
Schroeder, Daniel R.
Singh, Anil K.
Nakanishi, Koji
An improved synthesis of photoaffinity labeled, optically active retinal derivatives is presented.A stable, easy to handle, glyoxalic acid 2,4,6-triisopropylphenylsulfonylhydrazone (TIPPS) reacts with 3-hydroxyretinal to give the diazoacetylretinal analog in satisfactory yield.
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