SYNTHESIS OF OPTICALLY ACTIVE 3-DIAZOACETYLRETINALS WITH TRIISOPROPYLPHENYLSULFONYLHYDRAZONE

DOI: 10.1016/S0040-4039(00)86036-0

Source and publish data:

Tetrahedron Letters p. 2275 - 2278 (1988)

Update date:2022-08-05

Topics:

Authors:

Ok, Hyun

Caldwell, Charles

Schroeder, Daniel R.

Singh, Anil K.

Nakanishi, Koji

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Article abstract of DOI:10.1016/S0040-4039(00)86036-0

An improved synthesis of photoaffinity labeled, optically active retinal derivatives is presented.A stable, easy to handle, glyoxalic acid 2,4,6-triisopropylphenylsulfonylhydrazone (TIPPS) reacts with 3-hydroxyretinal to give the diazoacetylretinal analog in satisfactory yield.

Full text of DOI:10.1016/S0040-4039(00)86036-0

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