Journal of the Chemical Society, Dalton Transactions p. 2297 - 2304 (1995)
Update date:2022-08-05
Topics:
Rodriguez-Argueelles, Maria C.
Battaglia, Luigi Pietro
Ferrari, Marisa Belicchi
Fava, Giovanna Gasparri
Pelizzi, Corrado
Pelosi, Giorgio
The reaction of chlorides and acetates of Fe(II), Ni(II), Cu(II) and Zn(II) with the polydentate ligand cyclohexane-1,2-dione bis(thiosemicarbazone) (H2L) led to the formation of some novel complexes which have been characterized by spectroscopic methods (NMR, IR).The crystal structures of the two compounds a water molecule in 1 or by a chlorine atom in 2.The ligand is dideprotonated in 1 and neutral in 2, so that in 1 a higher ?-delocalization is observed.
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