DETERMINATION OF CONFIGURATION OF MONOSACCHARIDES BY HPLC ON DIASTEREOISOMERIC 1-DEOXY-1-(N-ACETYL-α-METHYLBENZYLAMINO)ALDITOL ACETATES

DOI: 10.1246/cl.1981.943

Source and publish data:

Chemistry Letters p. 943 - 946 (1981)

Update date:2022-08-05

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Authors:

Oshima, Ryuchi

Kumanotani, Ju

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Article abstract of DOI:10.1246/cl.1981.943

Acyclic diastereoisomers, 1-deoxy-1-(N-acetyl-α-methylbenzyl-amino)alditol acetates, are readily obtained by reductive amination of sugars with chiral α-methylbenzylamine in the presence of sodium cyanoborohydride.Ten pairs of enantiomers of common monosaccharides are resolved by an adsorption HPLC on the diastereoisomers.

Full text of DOI:10.1246/cl.1981.943

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