Reactions with Phosphororganic Compounds XLVIII. On the Behaviour of cis-1,2-Diols towards TPP/DEAD

DOI: 10.1007/BF00905072

Source and publish data:

Monatshefte fur Chemie p. 1045 - 1054 (1981)

Update date:2022-09-26

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Authors:

Penz, Gottfried

Zbiral, Erich

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Article abstract of DOI:10.1007/BF00905072

Reaction of the vicinal diols of steroids 1, 5, 7, 10, 13, and 16 with TPP/DEAD yields both regio- and stereospecifically the oxosteroids 2, 6, 8, 11, 14, and 15 by displacement of an axial hydrogen and extrusion of TPPO besides the cholest-4-en-6-ols 9 a

Full text of DOI:10.1007/BF00905072

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