GEZIELTE SYNTHESEN FUER BOROXAZINE

DOI: 10.1016/0022-328X(85)80026-7

Source and publish data:

Journal of Organometallic Chemistry p. 281 - 290 (1985)

Update date:2022-09-26

Topics:

Authors:

Oesterle, Rainer

Maringgele, Walter

Meller, Anton

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Article abstract of DOI:10.1016/0022-328X(85)80026-7

Cyclo-1-oxa-3,5-diaza-2,4,6-triboranes (A) and cyclo-1,3-dioxa-5-aza-2,4,6-triboranes (B) have been prepared by four different methods: (1) from mixtures of hexamethyldisilazanes and hexamethyldisiloxane with CH3BBr2 (A and B); (2) from (CH3)3SiN2 and CH3BBr2 (B); (3) from cyclo-1-oxa-3,5-diaza-2,4,6-trisilanes and CH3BBr2 (A); and (4) from CH3B2 and hexamethyldisiloxane (A).The products and some by-products were characterized by mass and NMR (1H, 11B, 29Si) spectra.Substances which were separated from the by-products were also analysed.

Full text of DOI:10.1016/0022-328X(85)80026-7

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