Crystal Structure of Fluoro(2,3,7,8,12,13,17,18-octaethylporphyrinato)oxoniobium; Demonstration of the Presence of Six-co-ordinated Niobium

DOI: 10.1039/DT9820000247

Source and publish data:

Journal of the Chemical Society, Dalton Transactions p. 247 - 250 (1982)

Update date:2022-07-30

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Authors:

Lecomte, Claude

Protas, Jean

Richard, Philippe

Barbe, Jean Michel

Guilard, Roger

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Article abstract of DOI:10.1039/DT9820000247

When HF is bubbled through a solution of (L=porphyrinate), porphyrinatoniobium oxide fluoride complexes are formed.The structures of some of these complexes have been studied from analytical and spectroscopic data.The title compound has been determined by X-ray diffraction methods.Crystals are monoclinic space group P2₁/c with a=15.007(3), b=22.257(4), c=10.058(2) Angstroem, β=77.85(2) deg, and Z=4.

Full text of DOI:10.1039/DT9820000247

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