Journal of Organic Chemistry p. 1931 - 1934 (1984)
Update date:2022-08-05
Topics:
Maricich, Tom J.
Angeletakis, Christos N.
Reaction of benzenesulfinyl azide (1) with thiols at -20 deg C gave thiosulfinates and hydrazoic acid.Reaction of 1 with primary and secondary amines gave sulfinamides and hydrazoic acid.The presence of a hydroxyl group in the thiol or amine did not change the course of the reaction.Thus, a thiosulfinate and sulfinamide containing a free hydroxyl group could be prepared.Yields ranging from 41percent to 93percent were obtained.
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